ｻﾝﾌﾟﾙ: '191024 Sample ﾌｧｲﾙ名: 191024　10μg エぴカテキン.FD3 分析日時: '10:12:57, 10/24/2019 ｵﾍﾟﾚｰﾀ: 筑波大学 ｺﾒﾝﾄ: ' 光度計 ﾓﾃﾞﾙ: F-7000形分光蛍光光度計 ｼﾘｱﾙ No.: 2357-015 ROM Ver.: 5J14000 06 装置条件 測定ﾓｰﾄﾞ: 3次元 ﾃﾞｰﾀﾓｰﾄﾞ: 蛍光 励起開始波長: 200.0 nm 励起終了波長: 500.0 nm 励起側ｻﾝﾌﾟﾘﾝｸﾞ間隔: 10.0 nm 蛍光開始波長: 200.0 nm 蛍光終了波長: 700.0 nm 蛍光側ｻﾝﾌﾟﾘﾝｸﾞ間隔: 10.0 nm ｽｷｬﾝｽﾋﾟｰﾄﾞ: 30000 nm/min 励起側ｽﾘｯﾄ: 5.0 nm 蛍光側ｽﾘｯﾄ: 5.0 nm ﾎﾄﾏﾙ電圧: 700 V ﾚｽﾎﾟﾝｽ: 自動 ｽﾍﾟｸﾄﾙ補正: On ｼｬｯﾀ制御: On 等高線間隔: 50.000 装置関数 励起側(200〜500nm) ｽﾘｯﾄ：5.0/20.0nm ﾎﾄﾏﾙ電圧：400V 蛍光側(200〜500nm) ｽﾘｯﾄ：5.0/20.0nm ﾎﾄﾏﾙ電圧：250V 蛍光側(500〜900nm) ｽﾘｯﾄ：---/5.0nm ﾎﾄﾏﾙ電圧：400V 励起側(500〜900nm) ｽﾘｯﾄ：5.0/5.0nm ﾎﾄﾏﾙ電圧：350V ﾃﾞｰﾀﾘｽﾄ 200.000 210.000 220.000 230.000 240.000 250.000 260.000 270.000 280.000 290.000 300.000 310.000 320.000 330.000 340.000 350.000 360.000 370.000 380.000 390.000 400.000 410.000 420.000 430.000 440.000 450.000 460.000 470.000 480.000 490.000 500.000 200.0 9999.9 5119 52.92 22.48 19.44 20.27 16.16 13.71 16.11 13.99 13.13 11.36 10.93 9.801 8.040 8.302 7.294 6.575 6.610 7.443 32.47 38.52 4.706 3.541 3.268 3.730 3.333 2.486 2.700 2.594 2.353 210.0 556.3 9999.9 3014 29.43 17.56 12.97 11.63 10.84 8.504 9.409 8.854 7.216 6.468 6.551 5.094 5.643 4.662 4.029 4.473 3.411 4.040 6.847 39.79 43.65 3.466 2.279 1.770 1.511 1.598 1.764 1.714 220.0 74.72 557.2 9999.9 2352 17.73 14.01 10.04 8.342 8.722 6.858 5.979 5.647 4.983 4.805 3.875 3.323 2.916 3.057 2.696 2.417 1.982 2.249 3.266 6.838 51.77 51.10 2.795 1.296 1.154 1.158 1.007 230.0 84.26 123.4 622.5 9999.9 2529 20.44 10.29 8.603 6.078 5.258 5.140 4.449 4.172 3.922 3.498 2.696 2.783 2.417 2.461 2.020 1.897 1.729 1.484 1.499 3.246 9.683 90.57 71.46 3.200 0.969 0.955 240.0 85.05 103.9 140.9 627.0 9999.9 3101 22.49 11.60 8.033 6.275 5.667 4.598 4.079 3.848 3.394 2.627 2.482 2.121 2.180 2.013 1.673 1.423 1.372 1.308 1.269 1.652 4.510 17.58 196.3 152.9 5.050 250.0 151.7 126.2 112.0 142.7 671.5 9999.9 3578 24.36 13.00 9.055 6.672 4.944 4.167 3.613 3.523 2.561 2.622 2.392 2.316 1.995 1.855 1.691 1.272 1.232 1.211 1.077 1.341 1.756 8.535 41.53 377.9 260.0 231.2 132.6 103.9 77.85 151.1 709.2 9999.9 3759 25.13 14.10 8.669 7.185 5.471 4.545 4.119 3.156 2.923 2.948 2.531 1.921 1.769 1.785 1.570 1.461 1.502 1.279 1.195 1.240 1.708 2.780 15.65 270.0 311.2 234.0 129.5 74.52 64.45 137.4 684.8 9999.9 3961 28.77 15.18 9.655 6.866 5.698 4.711 3.871 3.569 3.023 2.840 2.435 2.042 2.019 1.703 1.537 1.469 1.399 1.312 1.113 1.235 1.512 2.199 280.0 496.1 438.3 306.1 183.1 87.59 80.29 135.9 761.5 9999.9 3734 31.77 16.50 10.91 7.192 5.697 4.654 4.092 3.769 3.287 3.167 2.719 2.205 2.167 2.031 1.929 1.740 1.703 1.426 1.612 1.478 1.815 290.0 3090 3674 3294 2754 1013 325.3 695.6 1447 2285 9999.9 3794 36.60 19.23 11.51 8.337 6.140 5.372 4.932 4.254 4.227 4.449 4.597 5.018 4.899 5.473 6.362 7.232 6.114 4.951 3.283 3.195 300.0 8439 9999.9 9737 8345 3022 951.8 1990 4329 5122 2283 9999.9 3607 39.02 21.92 13.67 8.918 7.707 5.769 5.725 6.650 7.916 9.240 10.01 11.12 12.95 15.92 19.88 16.13 12.39 6.762 6.892 310.0 9999.9 9999.9 9999.9 9999.9 4283 1333 2825 6173 7426 2296 880.3 9999.9 3544 43.58 23.34 15.59 9.883 7.961 7.888 8.502 10.83 11.60 14.04 15.54 17.92 22.39 27.61 23.23 18.07 9.410 8.837 320.0 9999.9 9999.9 9999.9 9999.9 4227 1326 2803 6049 7260 2331 173.9 825.3 9999.9 3685 44.68 25.42 15.40 10.74 9.328 9.757 11.10 12.90 14.47 16.10 18.71 22.61 27.11 23.11 18.30 9.544 8.676 330.0 9259 9999.9 9999.9 9311 3350 1052 2203 4705 5647 1802 174.7 103.4 730.6 9999.9 3549 46.97 24.47 16.06 11.88 10.22 11.09 11.41 12.91 14.81 15.48 18.72 21.81 18.87 15.00 8.130 7.732 340.0 6825 8323 7682 6690 2493 843.2 1566 3228 3900 1312 133.9 100.3 105.3 672.5 9999.9 3597 46.43 24.43 16.13 12.60 10.96 11.28 11.34 11.73 12.95 14.74 16.93 14.23 11.15 7.133 7.294 350.0 4497 5670 5049 4442 1719 660.2 1079 2082 2475 889.5 109.7 105.7 85.46 103.9 664.8 9999.9 3576 45.08 24.41 16.53 12.82 11.02 10.21 10.19 10.47 11.36 12.84 10.99 8.875 6.535 6.208 360.0 3173 3419 3163 2766 1163 508.4 705.1 1263 1492 583.6 95.31 73.37 114.2 75.45 92.95 620.2 9999.9 3619 45.05 23.96 16.32 12.71 10.33 9.338 9.221 9.117 9.700 8.039 7.316 5.085 5.296 370.0 2419 2375 2044 1747 808.5 369.0 472.1 778.8 893.8 370.6 82.70 68.12 73.07 107.3 61.79 79.26 588.2 9999.9 3588 43.38 23.27 16.59 11.53 8.676 8.881 8.414 8.404 6.519 6.581 5.234 5.150 380.0 1693 1619 1399 1133 533.0 285.2 312.7 474.9 532.3 239.1 70.18 63.02 63.53 64.85 74.25 45.27 70.84 575.5 9999.9 3523 42.08 21.70 15.08 11.48 8.123 8.185 7.644 6.130 5.438 5.228 4.683 390.0 9410 1155 921.1 722.1 399.5 224.4 225.6 302.6 327.4 160.1 61.72 56.99 59.65 56.26 60.31 54.83 43.75 72.66 581.2 9999.9 3692 43.10 21.71 14.77 10.65 7.614 6.993 5.824 5.549 4.838 5.095 400.0 9999.9 979.4 671.0 497.5 303.5 210.8 163.0 207.4 216.1 111.7 54.45 51.68 51.31 50.31 45.70 58.53 42.67 44.03 74.20 579.6 9999.9 3720 40.79 20.67 13.54 9.983 7.211 6.414 5.424 4.974 4.716 410.0 2875 9999.9 512.2 365.3 246.4 187.7 127.5 144.1 139.2 81.61 48.53 43.91 44.38 44.22 40.73 40.51 54.60 37.25 39.80 68.86 552.7 9999.9 3881 38.32 19.16 13.19 8.648 7.222 5.545 5.681 4.982 420.0 934.4 9999.9 434.6 267.7 216.5 179.1 105.4 102.5 101.3 63.76 41.34 39.45 39.50 38.22 35.72 36.46 35.34 48.54 32.21 34.61 55.87 545.3 9999.9 3786 36.62 18.13 12.65 8.509 7.214 5.976 5.570 430.0 868.0 4726 9999.9 251.2 191.1 163.7 93.70 78.76 78.01 51.76 38.88 37.04 34.89 33.51 33.65 31.82 30.38 34.20 35.90 26.24 26.26 52.87 537.5 9999.9 3608 35.20 17.70 11.12 8.364 7.048 6.418 440.0 848.8 682.4 9999.9 229.1 171.7 154.8 83.43 70.54 61.20 46.27 33.55 33.54 31.78 30.37 29.56 31.95 28.50 25.18 32.05 26.72 22.12 25.00 50.96 559.5 9999.9 3437 33.74 16.22 11.21 8.230 6.962 450.0 770.5 519.3 4997 9999.9 144.8 162.1 81.07 57.26 53.23 39.74 33.31 30.65 29.74 28.95 30.43 31.65 27.95 23.51 23.61 31.04 21.31 20.99 23.74 53.01 560.2 9999.9 3311 32.47 17.49 11.82 8.886 460.0 868.3 533.7 529.5 9999.9 186.0 149.2 82.61 53.42 47.43 37.65 32.37 29.56 28.68 26.47 27.81 30.80 27.43 23.18 21.48 22.11 26.75 18.93 19.49 23.86 51.31 529.0 9999.9 3452 34.13 17.44 12.18 470.0 833.8 626.3 363.9 5500 9999.9 159.1 87.78 50.07 44.57 36.22 30.59 28.07 27.06 26.42 27.68 29.95 25.07 21.75 20.63 19.22 20.91 24.19 22.38 25.36 26.40 50.88 543.9 9999.9 3972 36.26 19.69 480.0 693.9 467.8 334.2 392.9 9999.9 191.7 80.29 50.21 41.39 35.44 29.46 26.61 26.09 24.61 25.18 27.38 24.27 21.21 18.75 17.87 18.44 22.18 18.82 17.21 19.13 21.15 47.00 500.0 9999.9 4119 36.50 490.0 728.5 467.3 278.3 201.9 6488 9999.9 88.85 50.03 37.66 34.07 30.81 26.02 22.83 21.51 24.17 24.78 21.60 17.35 17.14 16.77 15.45 15.50 20.97 15.87 16.41 17.29 18.93 41.76 494.0 9999.9 4697 500.0 551.9 489.8 250.7 183.5 387.2 9999.9 138.9 51.82 39.85 32.14 26.96 23.31 23.89 21.63 21.55 23.05 18.79 15.99 15.25 14.22 14.39 13.93 15.09 19.05 14.93 14.68 14.52 16.51 41.46 499.5 9999.9 510.0 673.1 407.9 238.5 160.4 132.6 7581 9999.9 61.59 39.89 32.46 27.74 24.31 21.49 19.83 21.33 19.25 18.53 15.69 12.93 12.62 13.21 12.91 13.33 14.23 16.01 12.21 12.28 13.23 17.20 41.02 486.8 520.0 692.2 355.8 236.1 111.9 148.6 415.5 9999.9 105.3 45.20 33.27 27.20 23.81 22.16 19.58 18.94 19.34 16.91 14.63 12.79 12.15 11.78 11.67 12.18 12.18 14.49 12.61 10.84 10.76 13.50 17.04 41.54 530.0 554.7 372.4 195.0 120.7 124.9 124.0 8092 9999.9 57.48 35.69 27.57 23.27 23.26 20.76 18.11 18.23 16.03 13.19 12.11 12.26 10.45 11.50 11.14 10.58 11.55 14.04 10.81 10.19 11.11 13.53 17.93 540.0 563.0 435.0 222.4 121.4 99.56 127.7 404.7 9999.9 111.3 44.17 32.82 26.03 22.76 21.56 19.75 17.95 15.85 11.68 11.00 10.91 10.47 10.78 10.18 11.27 9.227 10.90 12.17 9.882 9.984 11.50 12.91 550.0 632.3 436.1 202.6 108.0 81.73 128.1 91.23 9028 9999.9 57.77 38.41 26.49 22.00 20.95 20.27 17.97 15.97 12.27 10.70 10.66 10.05 9.422 8.670 9.128 10.26 9.891 10.45 10.38 9.443 9.843 11.90 560.0 740.2 441.5 257.3 133.8 97.47 86.57 88.98 436.1 9999.9 106.9 45.38 29.75 24.77 21.03 19.59 17.37 15.36 13.11 12.25 10.27 9.968 10.16 8.679 8.508 8.159 9.870 9.070 10.50 9.057 8.379 10.42 570.0 858.2 669.2 473.1 357.9 145.8 91.69 148.9 184.6 9191 9999.9 58.25 35.67 26.89 21.60 20.02 17.42 15.19 13.78 13.69 10.34 8.897 10.13 9.970 8.390 8.434 8.399 9.612 9.070 11.31 8.600 10.00 580.0 1978 1631 1419 1097 414.4 179.2 298.3 566.1 1019 9999.9 117.1 46.17 31.16 24.44 20.59 18.97 16.42 14.31 12.95 15.03 9.358 10.69 10.16 9.352 8.986 8.821 9.404 9.614 10.22 9.945 9.109 590.0 7712 3017 2602 2244 823.3 297.9 541.5 1159 1363 9999.9 9999.9 62.89 37.47 27.04 22.00 20.55 16.80 15.92 14.30 13.00 12.63 12.02 10.66 10.92 10.40 10.55 11.70 11.00 9.943 11.61 10.98 600.0 9999.9 4361 3810 3352 1147 391.5 789.5 1682 1986 1015 9999.9 109.0 45.02 31.60 25.30 21.48 17.30 17.37 14.12 12.32 18.34 13.41 11.38 12.29 10.76 11.63 13.49 12.88 11.39 10.45 12.55 610.0 7741 5799 4780 4027 1415 483.6 984.6 2068 2436 790.6 9999.9 9999.9 57.88 38.58 26.88 23.03 19.31 16.88 14.62 13.34 12.99 19.56 13.53 11.79 11.96 13.06 14.20 13.28 11.58 9.103 11.94 620.0 5158 9999.9 5006 4333 1549 518.5 1074 2226 2697 818.9 488.3 9999.9 98.50 43.27 31.36 24.26 18.50 16.99 16.45 14.63 13.31 17.10 15.93 13.23 14.39 14.80 16.04 13.52 11.76 8.541 9.726 630.0 4310 9999.9 5041 4224 1550 507.6 1018 2228 2674 841.7 106.8 9999.9 9999.9 59.82 38.44 29.74 23.53 19.65 20.07 15.20 13.24 14.20 25.95 13.55 14.74 15.25 15.95 14.44 13.01 8.445 8.702 640.0 4010 9952 4894 4016 1490 493.9 965.1 2017 2451 820.3 88.68 466.1 9999.9 111.9 46.61 35.76 25.97 18.89 17.69 16.45 15.75 14.14 16.13 24.67 15.79 16.25 16.36 12.32 11.66 7.918 8.137 650.0 4100 5083 8332 3582 1264 416.3 814.8 1793 2205 727.4 78.12 78.65 9999.9 9999.9 58.77 40.02 29.40 24.58 21.85 16.66 17.92 16.08 14.98 22.57 18.01 14.94 15.32 12.96 12.38 7.689 8.104 660.0 3754 4262 9999.9 3119 1190 380.1 730.6 1593 1891 636.3 78.58 62.27 463.3 9999.9 108.1 48.23 33.96 29.13 25.40 22.08 18.35 18.16 17.32 14.97 39.22 15.18 15.73 13.28 11.63 9.282 8.278 670.0 3613 3743 8832 2854 990.7 321.1 648.1 1329 1594 534.8 96.13 54.55 87.76 9999.9 9999.9 60.94 44.18 31.92 28.05 24.38 21.07 19.52 18.32 16.74 18.66 28.27 15.25 12.21 11.64 8.218 9.952 680.0 2818 3296 3349 6070 866.4 326.0 560.9 1086 1302 451.6 71.88 65.87 65.30 469.9 9999.9 107.2 49.31 39.29 32.52 27.14 24.61 21.14 23.12 18.39 18.98 32.31 19.34 14.73 10.39 10.71 8.381 690.0 2502 2689 2219 9999.9 774.4 261.7 469.1 884.1 1044 374.4 66.26 84.07 61.26 92.29 9999.9 9999.9 66.30 45.92 34.97 32.53 27.38 23.77 22.44 20.38 17.81 18.79 59.84 12.90 11.43 11.26 9.777 700.0 2139 1998 2199 8763 790.1 259.8 385.7 708.9 833.5 310.1 62.75 71.83 55.52 62.99 478.9 9999.9 110.0 52.69 39.63 38.02 29.60 24.54 23.44 21.95 21.24 18.29 22.83 40.96 10.77 10.10 10.55